BS EN 17250:2020
Foodstuffs. Determination of ochratoxin A in spices, liquorice, cocoa and cocoa products by IAC clean-up and HPLC-FLD
Standard number: | BS EN 17250:2020 |
Pages: | 30 |
Released: | 2020-01-30 |
ISBN: | 978 0 580 98502 7 |
Status: | Standard |
BS EN 17250:2020
This standard BS EN 17250:2020 Foodstuffs. Determination of ochratoxin A in spices, liquorice, cocoa and cocoa products by IAC clean-up and HPLC-FLD is classified in these ICS categories:
- 67.220.10 Spices and condiments
- 67.140.30 Cocoa
This document specifies a procedure for the determination of ochratoxin A (OTA) in chilli, paprika, black and white pepper, nutmeg, spice mix, liquorice (root and extracts), cocoa and cocoa products by high performance liquid chromatography (HPLC) with immunoaffinity column clean-up and fluorescence detection (FLD).
This method has been validated in interlaboratory studies via the analysis of both naturally contaminated and spiked samples ranging from 1,0 ?g/kg to 84,9 ?g/kg for spices (paprika and chili [5], black and white pepper, nutmeg and spice mix [6]), ranging from 7,7 ?g/kg to 96,8 ?g/kg for liquorice and liquorice products [7] and ranging from 2,1 ?g/kg to 26,3 ?g/kg for cocoa and cocoa products [6].
For further information on the validation, see Clause 10 and Annex B.