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Homepage>BS Standards>67 FOOD TECHNOLOGY>67.060 Cereals, pulses and derived products>BS EN 17280:2019 Foodstuffs. Determination of zearalenone and trichothecenes including deoxynivalenol and its acetylated derivatives (3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol), nivalenol T-2 toxin and HT-2 toxin in cereals and cereal products by LC-MS/MS
immediate downloadReleased: 2019-10-17
BS EN 17280:2019 Foodstuffs. Determination of zearalenone and trichothecenes including deoxynivalenol and its acetylated derivatives (3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol), nivalenol T-2 toxin and HT-2 toxin in cereals and cereal products by LC-MS/MS

BS EN 17280:2019

Foodstuffs. Determination of zearalenone and trichothecenes including deoxynivalenol and its acetylated derivatives (3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol), nivalenol T-2 toxin and HT-2 toxin in cereals and cereal products by LC-MS/MS

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Standard number:BS EN 17280:2019
Pages:52
Released:2019-10-17
ISBN:978 0 539 00386 4
Status:Standard
BS EN 17280:2019 - Foodstuffs Analysis Standard

BS EN 17280:2019 - Comprehensive Analysis of Mycotoxins in Cereals

Ensure the safety and quality of your cereal products with the BS EN 17280:2019 standard. This essential document provides a detailed methodology for the determination of zearalenone and trichothecenes, including deoxynivalenol and its acetylated derivatives, nivalenol, T-2 toxin, and HT-2 toxin in cereals and cereal products using the advanced LC-MS/MS technique.

Key Features of BS EN 17280:2019

  • Standard Number: BS EN 17280:2019
  • Pages: 52
  • Release Date: October 17, 2019
  • ISBN: 978 0 539 00386 4
  • Status: Standard

Why Choose BS EN 17280:2019?

In the food industry, ensuring the safety of products is paramount. Mycotoxins such as zearalenone and trichothecenes pose significant health risks, and their presence in foodstuffs must be accurately monitored and controlled. The BS EN 17280:2019 standard provides a robust framework for laboratories and food manufacturers to detect and quantify these harmful substances, ensuring compliance with safety regulations and protecting consumer health.

Advanced Analytical Techniques

The standard employs Liquid Chromatography coupled with Tandem Mass Spectrometry (LC-MS/MS), a cutting-edge analytical technique known for its precision and sensitivity. This method allows for the accurate detection of even trace levels of mycotoxins, providing reliable results that you can trust.

Comprehensive Coverage

BS EN 17280:2019 covers a wide range of mycotoxins, including:

  • Zearalenone
  • Deoxynivalenol and its acetylated derivatives (3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol)
  • Nivalenol
  • T-2 toxin
  • HT-2 toxin

This comprehensive coverage ensures that all major mycotoxins of concern in cereals and cereal products are addressed, providing peace of mind for producers and consumers alike.

Industry Relevance

Released in 2019, this standard reflects the latest scientific advancements and regulatory requirements. It is an indispensable resource for food safety professionals, quality assurance teams, and laboratory technicians working in the cereal and grain industry.

Benefits of Implementing BS EN 17280:2019

By adopting this standard, organizations can achieve several key benefits:

  • Enhanced Food Safety: Protect consumers by ensuring that cereal products are free from harmful levels of mycotoxins.
  • Regulatory Compliance: Meet national and international food safety standards and regulations, avoiding potential legal and financial repercussions.
  • Improved Product Quality: Maintain high-quality standards for cereal products, enhancing brand reputation and consumer trust.
  • Competitive Advantage: Stand out in the market by demonstrating a commitment to food safety and quality assurance.

Who Should Use This Standard?

BS EN 17280:2019 is designed for a wide range of stakeholders in the food industry, including:

  • Food Safety Managers
  • Quality Assurance Professionals
  • Laboratory Technicians
  • Regulatory Compliance Officers
  • Food Manufacturers and Processors

Whether you are involved in the production, testing, or regulation of cereal products, this standard provides the guidance needed to ensure the highest levels of safety and quality.

Conclusion

In an industry where safety and quality are non-negotiable, the BS EN 17280:2019 standard is an invaluable tool. By providing a detailed methodology for the detection and quantification of mycotoxins in cereals, it helps organizations safeguard consumer health, comply with regulations, and maintain product excellence. Invest in this standard to enhance your food safety protocols and protect your brand's reputation.

DESCRIPTION

BS EN 17280:2019


This standard BS EN 17280:2019 Foodstuffs. Determination of zearalenone and trichothecenes including deoxynivalenol and its acetylated derivatives (3-acetyl-deoxynivalenol and 15-acetyl-deoxynivalenol), nivalenol T-2 toxin and HT-2 toxin in cereals and cereal products by LC-MS/MS is classified in these ICS categories:
  • 67.060 Cereals, pulses and derived products

This document specifies a procedure for the determination of nivalenol (NIV), deoxynivalenol (DON) and its acetyl derivatives (3-acetyl-DON and 15-acetyl-DON), HT-2 and T-2 toxins (HT-2 and T-2) and zearalenone (ZEN) in cereals and cereal products by high performance liquid chromatography (HPLC) coupled with tandem mass spectrometry (MS/MS) after clean-up by solid phase extraction (SPE).

The method has been validated with samples of wheat, wheat flour, and wheat crackers. The wheat and the wheat flour were prepared from a mixture of wheat and fungi infected wheat kernels. The wheat crackers were baked from wheat flour and water spiked with the target mycotoxins.

Validation levels for NIV ranged from 27,7 ?g/kg to 378 ?g/kg.

Validation levels for DON ranged from 234 ?g/kg to 2420 ?g/kg.

Validation levels for 3-acetyl-DON ranged from 18,5 ?g/kg to 137 ?g/kg.

Validation levels for 15-acetyl-DON ranged from 11,4 ?g/kg to 142 ?g/kg.

Validation levels for HT-2 ranged from 6,6 ?g/kg to 134 ?g/kg.

Validation levels for T-2 ranged from 2,1 ?g/kg to 37,6 ?g/kg.

Validation levels for ZEN ranged from 31,6 ?g/kg to 230 ?g/kg.

Laboratory experiences have shown that this method is also applicable to barley and oat flour, and rye based crackers [5], however, this has not been validated in a collaborative study.