Tracked Changes. Animal and vegetable fats and oils. Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol
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Standard number:
BS EN ISO 18363-3:2024 - TC
Pages:
58
Released:
2024-07-30
ISBN:
978 0 539 32685 7
Status:
Tracked Changes
DESCRIPTION
BS EN ISO 18363-3:2024 - TC
This standard BS EN ISO 18363-3:2024 - TC Tracked Changes. Animal and vegetable fats and oils. Determination of fatty-acid-bound chloropropanediols (MCPDs) and glycidol by GC/MS is classified in these ICS categories:
67.200.10 Animal and vegetable fats and oils
This document specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2-MCPD), 3?MCPD esters (bound 3?MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. This document is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg.
