Animal and vegetable fats and oils - Determination of fattyacid- bound chloropropanediols (MCPDs) and glycidol by GC/MS - Part 3: Method using acid transesterification and measurement for 2-MCPD, 3-MCPD and glycidol
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Number of Standard:
CSN EN ISO 18363-3
Category:
588725
Pages:
32
Released:
01.01.2025
Catalog number:
520297
DESCRIPTION
CSN EN ISO 18363-3
CSN EN ISO 18363-3 This document specifies a procedure for the simultaneous determination of 2-MCPD esters (bound 2 MCPD), 3-MCPD esters (bound 3-MCPD) and glycidyl esters (bound glycidol) in a single assay, based on acid catalysed ester cleavage and derivatization of cleaved (free) analytes with phenylboronic acid (PBA) prior to GC/MS analysis. This document is applicable to solid and liquid fats and oils. For all three analytes the limit of quantification (LOQ) is 0,1 mg/kg and the limit of detection (LOD) is 0,03 mg/kg. Original English text of CSN EN Standard. The price of the Standard included all amendments and correcturs.
